（毕业设计论文）《ESE中黄酮类物质稳定性研究》.docVIP

本 科 生 毕 业 设 计 (论 文) 题目：ESE中黄酮类物质稳定性研究 Study on the Stability of Flavonoids from ESE 教学单位 化学与环境保护工程学院 姓 名 _ _______ 学 号 _ 200831205010____ 年 级 _______2008 级_______ 专 业 ____ 制药工程专业_ 指导教师 ___ 职 称 ___ 教 授 2012年 05月 04日 目录 摘要···································································3 引言···································································5 1.材料与方法···························································6 1.1材料·····························································6 1.1.1供试原料·····················································6 1.1.2主要化学试剂·················································6 1.1.3主要仪器及设备···············································6 1.2方法·····························································6 1.2.1水解溶液配置·················································6 1.2.2黄酮药粉水解工艺流程·········································7 1.2.3正交试验条件·················································7 1.2.4黄酮药粉水解方法·············································7 1.2.5重复试验·····················································7 1.2.6终试放大试验·················································7 2.结果与分析···························································7 2.1正交试验·························································8 2.1.1正交试验结果·················································8 2.1.2结果分析·····················································8 2.2原始数据记录·····················································8 2.2.1正交试验水解反应数据·········································8 2.2.2取样TLC鉴定数据·············································9 2.2.3点样结论·····················································9 2.2.4物理水提法洗涤沉淀···········································9 2.2.5洗涤后沉淀记录及鉴定·········································10 2.2.6洗涤结论·····················································10 2.3重复试验原始数据记录·············································10 2.3.1 A3B2