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本 科 生 毕 业 设 计 (论 文)
题目:ESE中黄酮类物质稳定性研究
Study on the Stability of Flavonoids from ESE
教学单位 化学与环境保护工程学院
姓 名 _ _______
学 号 _ 200831205010____
年 级 _______2008 级_______
专 业 ____ 制药工程专业_
指导教师 ___
职 称 ___ 教 授
2012年 05月 04日
目录
摘要···································································3
引言···································································5
1.材料与方法···························································6
1.1材料·····························································6
1.1.1供试原料·····················································6
1.1.2主要化学试剂·················································6
1.1.3主要仪器及设备···············································6
1.2方法·····························································6
1.2.1水解溶液配置·················································6
1.2.2黄酮药粉水解工艺流程·········································7
1.2.3正交试验条件·················································7
1.2.4黄酮药粉水解方法·············································7
1.2.5重复试验·····················································7
1.2.6终试放大试验·················································7
2.结果与分析···························································7
2.1正交试验·························································8
2.1.1正交试验结果·················································8
2.1.2结果分析·····················································8
2.2原始数据记录·····················································8
2.2.1正交试验水解反应数据·········································8
2.2.2取样TLC鉴定数据·············································9
2.2.3点样结论·····················································9
2.2.4物理水提法洗涤沉淀···········································9
2.2.5洗涤后沉淀记录及鉴定·········································10
2.2.6洗涤结论·····················································10
2.3重复试验原始数据记录·············································10
2.3.1 A3B2
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